Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (7): 1095-1104.DOI: 10.1007/s40195-021-01370-7
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Xu Lu1, Dong Wang1, Di Wan1, Xiaofei Guo2,3, Roy Johnsen1
Received:
2021-09-10
Revised:
2021-11-05
Accepted:
2021-11-19
Online:
2023-07-10
Published:
2023-07-04
Xu Lu, Dong Wang, Di Wan, Xiaofei Guo, Roy Johnsen. Reveal Hydrogen Behavior at Grain Boundaries in Fe-22Mn-0.6C TWIP Steel via In Situ Micropillar Compression Test[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(7): 1095-1104.
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C | Mn | Al | Nb | V | Ti | N | Fe |
---|---|---|---|---|---|---|---|
0.63 | 22.60 | 0.008 | 0.03 | 0.108 | 0.03 | 0.016 | Bal. |
Table 1 Chemical composition of the studied TWIP steel
C | Mn | Al | Nb | V | Ti | N | Fe |
---|---|---|---|---|---|---|---|
0.63 | 22.60 | 0.008 | 0.03 | 0.108 | 0.03 | 0.016 | Bal. |
GB | Grain A | Grain B | [U V W] | θ | α |
---|---|---|---|---|---|
(φ1 Φ φ2) | |||||
LAGB1 | (270.2 89.2 179.6) | (86.8 91.3 2.2) | [− 1 - 10 5] | 4.2° | 90° |
LAGB2 | (355.7 4.5 301.3) | (291.6 92.5 181.4) | [− 1 17 15] | 7.8° | 50.1° |
HAGB1 | (263.7 82.5 176.0) | (134.2 32.4 71.1) | [− 12 17 14] | 43.4° | 89.2° |
HAGB2 | (46.0 66.6 340.4) | (318.5 133.9 185.4) | [− 7 - 4 11] | 33.5° | 87.1° |
HAGB3 | (316.8 93.2 142.6) | (75.6 72.7 315.3) | [− 8 - 6 5] | 52.3° | 76.9° |
Table 2 Crystallographic information of the selected GBs ((φ1 Φ φ2) denotes Euler angles, α is the tilt angle between the sample surface and the GB, [U V W] is the misorientation axis, and θ is the misorientation angle between adjacent grains)
GB | Grain A | Grain B | [U V W] | θ | α |
---|---|---|---|---|---|
(φ1 Φ φ2) | |||||
LAGB1 | (270.2 89.2 179.6) | (86.8 91.3 2.2) | [− 1 - 10 5] | 4.2° | 90° |
LAGB2 | (355.7 4.5 301.3) | (291.6 92.5 181.4) | [− 1 17 15] | 7.8° | 50.1° |
HAGB1 | (263.7 82.5 176.0) | (134.2 32.4 71.1) | [− 12 17 14] | 43.4° | 89.2° |
HAGB2 | (46.0 66.6 340.4) | (318.5 133.9 185.4) | [− 7 - 4 11] | 33.5° | 87.1° |
HAGB3 | (316.8 93.2 142.6) | (75.6 72.7 315.3) | [− 8 - 6 5] | 52.3° | 76.9° |
Fig. 1 a Microstructure of the studied TWIP steel showing the selected GB for micropillar fabrication; b the corresponding inverse pole figure (IPF) map; c SEM image of FIB-milled micropillars along the GB marked in a; d higher magnification of the pristine micropillar enclosed by the yellow box in c
Fig. 2 Representative a engineering stress-strain curves; b stress-strain curves in the elastic regime for micropillars at LAGB2 that were tested in both hydrogen-free and hydrogen-charged conditions
Fig. 6 Micrographs of the micropillar lamellae containing HAGB3 after compressed in a1 air, b1 hydrogen-charged conditions; and the corresponding t-EBSD results showing a2, b2 IPF, a3, b3 image quality (IQ) maps
Fig. 7 Bright-field STEM images showing dislocations and twins in the deformed micropillars from HAGB3 tested in a hydrogen-free, b hydrogen-charged conditions. The yellow arrows refer to twins, and the red arrows refer to dislocations
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