Acta Metallurgica Sinica (English Letters) ›› 2021, Vol. 34 ›› Issue (12): 1695-1703.DOI: 10.1007/s40195-021-01232-2

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Effects of MeV Fe Ions Irradiation on the Microstructure and Property of Nuclear Grade 304 Stainless Steel: Characterized by Positron Annihilation Spectroscopy, Transmission Electron Microscope and Nanoindentation

Honglin Yan1,2, Zhiming Zhang1(), Jianqiu Wang1, Bright O. Okonkwo1,2, En-Hou Han1   

  1. 1Key Laboratory of Nuclear Materials and Safety Assessment, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
    2School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
  • Received:2020-11-09 Revised:2021-01-18 Accepted:2021-01-26 Online:2021-12-10 Published:2021-12-10
  • Contact: Zhiming Zhang
  • About author:Zhiming Zhang zmzhang@imr.ac.cn

Abstract:

Nuclear grade 304 stainless steel was irradiated by 3.5 MeV Fe ions, with fluxes of 3.05E+15 ions/cm2 and 1.55E+16 ions/cm2. Irradiation effects were studied by positron annihilation spectroscopy (PAS), transmission electron microscope (TEM) and nanoindentation techniques. PAS results showed that different types of defects were produced after irradiation and that there was significant variance in defects formed when the samples were subjected to different irradiation doses. TEM characterization showed that the irradiation-induced dislocation loops enlarged in average size, but decreased in number density at higher irradiation doses. Nanoindentation test showed obvious irradiation hardening phenomenon, which was in good agreement with the PAS and TEM results. Irradiation hardening effect increased with an increase in irradiation dose and saturation occurred with an increase in irradiation dose from 3.2 to 16 dpa. Further statistical analysis showed that barrier strength of the Frank loop depends on the loop size and density produced by the ion irradiation.

Key words: Stainless steel, Irradiation hardening, Positron annihilation, Nanoindentation