Acta Metallurgica Sinica (English Letters) ›› 2020, Vol. 33 ›› Issue (10): 1321-1330.DOI: 10.1007/s40195-020-01098-w
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Sami Bin Humam1, Gobinda Gyawali2(), Dhani Ram Dhakal1, Jin-Hyuk Choi1, Soo Wohn Lee1()
Received:
2020-04-10
Revised:
2020-05-11
Online:
2020-10-10
Published:
2020-10-20
Contact:
Gobinda Gyawali,Soo Wohn Lee
Sami Bin Humam, Gobinda Gyawali, Dhani Ram Dhakal, Jin-Hyuk Choi, Soo Wohn Lee. Effect of Pulse and Direct Current Electrodeposition on Microstructure, Surface, and Scratch Resistance Properties of Ni-W Alloy and Ni-W-SiC Composite Coatings[J]. Acta Metallurgica Sinica (English Letters), 2020, 33(10): 1321-1330.
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Composition | Concentration | Purpose |
---|---|---|
NiSO4·6H2O (mol) | 0.075 | Ni source |
Na2WO4·2H2O (mol) | 0.112 | W source |
Na3C6H5O7·H2O (mol) | 0.187 | Complexing agent |
NH4Cl (mol) | 0.5 | Buffer |
NaBr (mol) | 0.6 | Conductivity |
SDS (g/L) | 0.3 | Surfactant |
SiC particles (g/L) | 0,20 | Composite phase |
Table 1 Experimental bath formulation
Composition | Concentration | Purpose |
---|---|---|
NiSO4·6H2O (mol) | 0.075 | Ni source |
Na2WO4·2H2O (mol) | 0.112 | W source |
Na3C6H5O7·H2O (mol) | 0.187 | Complexing agent |
NH4Cl (mol) | 0.5 | Buffer |
NaBr (mol) | 0.6 | Conductivity |
SDS (g/L) | 0.3 | Surfactant |
SiC particles (g/L) | 0,20 | Composite phase |
Temperature (°C) | Electrodeposition time (min) | Current density (mA/cm2) | Stirring/agitation (rpm) | Anode | Cathode |
---|---|---|---|---|---|
65 | 60 | 80 | 180 | Graphite | Copper |
Table 2 Electrodeposition conditions
Temperature (°C) | Electrodeposition time (min) | Current density (mA/cm2) | Stirring/agitation (rpm) | Anode | Cathode |
---|---|---|---|---|---|
65 | 60 | 80 | 180 | Graphite | Copper |
Samples | Grain size (nm) | Lattice strain (%) |
---|---|---|
Ni-W DC | 12 | 0.0876 |
Ni-W PC | 8.5 | 0.1185 |
Ni-W-SiC DC | 9.2 | 0.1111 |
Ni-W-SiC PC | 9.1 | 0. 1124 |
Table 3 Grain size and lattice strain of Ni-W and Ni-W-SiC composite coatings
Samples | Grain size (nm) | Lattice strain (%) |
---|---|---|
Ni-W DC | 12 | 0.0876 |
Ni-W PC | 8.5 | 0.1185 |
Ni-W-SiC DC | 9.2 | 0.1111 |
Ni-W-SiC PC | 9.1 | 0. 1124 |
Samples | Ra (μm) | Rq (μm) | Rmax (μm) |
---|---|---|---|
Ni-W DC | 0.358 | 0.704 | 2.375 |
Ni-W PC | 0.224 | 0.344 | 1.677 |
Ni-W-SiC DC | 1.170 | 1.496 | 7.519 |
Ni-W-SiC PC | 0.735 | 0.920 | 4.324 |
Table 4 Surface roughness profiles of Ni-W and Ni-W-SiC composite coatings
Samples | Ra (μm) | Rq (μm) | Rmax (μm) |
---|---|---|---|
Ni-W DC | 0.358 | 0.704 | 2.375 |
Ni-W PC | 0.224 | 0.344 | 1.677 |
Ni-W-SiC DC | 1.170 | 1.496 | 7.519 |
Ni-W-SiC PC | 0.735 | 0.920 | 4.324 |
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