Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (12): 2013-2030.DOI: 10.1007/s40195-023-01608-6
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Hongyang Cui1,2, Yi Tan1,2, Rusheng Bai1,2, Lidan Ning1,2, Chuanyong Cui3, Xiaogang You4, Pengting Li1,2()
Received:
2023-04-18
Revised:
2023-08-22
Accepted:
2023-08-23
Online:
2023-10-30
Published:
2023-10-30
Contact:
Pengting Li
Hongyang Cui, Yi Tan, Rusheng Bai, Lidan Ning, Chuanyong Cui, Xiaogang You, Pengting Li. Recrystallization Behavior of the New Ni-Co-Based Superalloy with Fusion Structure Produced by Electron Beam Smelting Layered Solidification Technology[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(12): 2013-2030.
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Co | Cr | W | Mo | Al + Ti | C + Zr + B | Ni |
---|---|---|---|---|---|---|
20-26 | 13-15 | 1.1-1.3 | 2.4-2.8 | 7.72-8.40 | 0.04-0.11 | Bal. |
Table 1 Main composition of Ni-Co-based superalloy (wt%)
Co | Cr | W | Mo | Al + Ti | C + Zr + B | Ni |
---|---|---|---|---|---|---|
20-26 | 13-15 | 1.1-1.3 | 2.4-2.8 | 7.72-8.40 | 0.04-0.11 | Bal. |
Fig. 1 Microstructures of the new Ni-Co-based superalloy: a-a3 cast microstructures of EBSL-Ni-Co-based superalloy; b-b3 homogenized state microstructures of EBSL-Ni-Co-based superalloy; c-c3 homogenized state microstructures of DM-Ni-Co-based superalloy, d DSC curves of the EBSL-Ni-Co superalloy, d1 microstructure of the alloy solution treatment at 1120 °C for 10 min, d2 microstructure of the alloy solution treatment at 1160 °C for 10 min
Fig. 2 a Sampling requirements diagram; b schematic diagram of hot compression process schematic diagram; c the directions of sampling and characterization for EBSD and TEM tests
Fig. 3 Microstructures of the alloy after heat treatment at 1150 °C for 4 h: a EBSL-Ni-Co superalloy, b DM-Ni-Co superalloy, c grain size distribution map, d misorientation angle distribution map
Fig. 4 Corrected true stress-strain curves of the new Ni-Co superalloy under the hot deformed: a 1120 °C of EBSL-Ni-Co superalloy, b 1160 °C of EBSL-Ni-Co superalloy, c various microstructure, d schematic representations of the flow stress curve
Fig. 5 Microstructural characteristics of the new Ni-Co-based superalloy deformed at γ′ super-solvus temperature (1160 °C) to a strain rate of 0.01 s−1 with different strains: a-d DM-Ni-Co superalloy, e-h EBSL-Ni-Co superalloy
Fig. 6 Microstructural characteristics of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperatures to a strain of 0.7 with different strain rates: a-d γ′ sub -solvus temperatures (1120 °C), e-h γ′ super-solvus temperatures (1160 °C)
Fig. 7 a DRX grain volume fraction of different microstructures, b evolution of dislocation density inside a recrystallized grain during the DRX process, c the kernel average misorientation map for different deformation strains
Fig. 8 Distributions of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperature to a strain of 0.7 with different strain rates: a volume fraction of DRX grain, b volume fraction of LAGBs, MAGBs and HAGBs
Fig. 9 a DRX grain size distributions of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperature to a strain of 0.7 with different strain rates, b schematic diagram of the interaction between a moving grain boundary and the dispersed γ′ phase, c, d microstructures at a strain rate of 0.01 s−1, e, f microstructures at a strain rate of 0.001 s−1
Fig. 10 Schematic diagram of the microstructure evolution deformed though DDRX: a IPF of regions G1 and the line graph, b misorientation angle along the arrow, c schematic diagram of microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphologies of the EBSL-Ni-Co superalloy
Fig. 11 Schematic diagram of the microstructure evolution deformed though CDRX: a IPF of regions G2, b the line graph and misorientation angle along the arrow, c microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphology of the EBSL-Ni-Co superalloy
Fig. 12 Schematic diagram of the microstructure evolution for the formation of TDRX: a, b IPF with strain 0.3, c microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphology of the EBSL- Ni-Co superalloy
Fig. 13 Schematic diagram of the microstructure evolution deformed though PSN: a, b TEM morphologies of the EBSL-Ni-Co superalloy, c microstructure deformed under EBSL-Ni-Co-based superalloy
Fig. 14 Schematic illustration of grain refinement evolution and corresponding mechanisms during hot compression deformation: a γ′ sub-solvus temperature (1120 °C), b γ′ super-solvus temperature (1160 °C)
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