Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (1): 61-76.DOI: 10.1007/s40195-022-01447-x
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Chunxiao Li1,2, Hong Yan1,3,*(), Rongshi Chen1,*(
)
Received:
2022-03-24
Revised:
2022-05-21
Accepted:
2022-06-09
Online:
2023-01-10
Published:
2022-08-16
Contact:
* Hong Yan,hyan@imr.ac.cn; Rongshi Chen,rschen@imr.ac.cn
Chunxiao Li, Hong Yan, Rongshi Chen. Microstructure and Texture Evolution of Mg-14Gd-0.5Zr Alloy during Rolling and Annealing under Different Temperatures[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(1): 61-76.
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Rolling temperature ( °C) | Sample number | Annealing treatment | Sample number |
---|---|---|---|
450 | R1 | 450 °C × 10 min | R1-450 °C |
475 °C × 10 min | R1-475 °C | ||
500 °C × 10 min | R1-500 °C | ||
475 | R2 | 450 °C × 10 min | R2-450 °C |
475 °C × 10 min | R2-475 °C | ||
500 °C × 10 min | R2-500 °C | ||
500 | R3 | 450 °C × 10 min | R3-450 °C |
475 °C × 10 min | R3-475 °C | ||
500 °C × 10 min | R3-500 °C |
Table 1 List of rolling temperature and annealing treatment of the samples
Rolling temperature ( °C) | Sample number | Annealing treatment | Sample number |
---|---|---|---|
450 | R1 | 450 °C × 10 min | R1-450 °C |
475 °C × 10 min | R1-475 °C | ||
500 °C × 10 min | R1-500 °C | ||
475 | R2 | 450 °C × 10 min | R2-450 °C |
475 °C × 10 min | R2-475 °C | ||
500 °C × 10 min | R2-500 °C | ||
500 | R3 | 450 °C × 10 min | R3-450 °C |
475 °C × 10 min | R3-475 °C | ||
500 °C × 10 min | R3-500 °C |
Fig. 2 Microstructures of GK140: a, b optical and SEM microstructure images of GK140 in the cast state; c, d optical and SEM microstructures of GK140 in the solution state; e EDS results of point A in b
Fig. 6 Optical microstructures of a-c R1-450 °C, R2-450 °C and R3-450 °C; d-f R1-475 °C, R2-475 °C and R3-475 °C; g-i R1-500 °C, R2-500 °C and R3-500 °C
Fig. 7 a-c Inverse pole figure maps of R1-500 °C, R2-500 °C and R3-500 °C; d-f KAM maps of R1-500 °C, R2-500 °C and R3-500 °C. Figures inserted in a-c are boundary maps with dashed rectangles
Variant 1 | Variant 2 | Variant 3 | Variant 4 | Variant 5 | Variant 6 | Strain accommodated | |
---|---|---|---|---|---|---|---|
R1 | 0.05 | 0.12 | 0.10 | 0.05 | 0.07 | 0.05 | 0.04 |
R2 | 0.23 | 0.28 | 0.04 | 0.26 | 0.29 | 0.01 | 0.01 |
R3 | 0.08 | 0.14 | - 0.23 | 0.07 | 0.12 | -0.25 | 0.02 |
Table 2 SF of extensive twin variant under the PSC condition and the strain accommodated by twinning
Variant 1 | Variant 2 | Variant 3 | Variant 4 | Variant 5 | Variant 6 | Strain accommodated | |
---|---|---|---|---|---|---|---|
R1 | 0.05 | 0.12 | 0.10 | 0.05 | 0.07 | 0.05 | 0.04 |
R2 | 0.23 | 0.28 | 0.04 | 0.26 | 0.29 | 0.01 | 0.01 |
R3 | 0.08 | 0.14 | - 0.23 | 0.07 | 0.12 | -0.25 | 0.02 |
Fig. 12 a High angle annular dark field image of grain boundaries in R2; b, c EDS maps corresponding to a; d high angle annular dark field image of grain boundaries in R3; e, f EDS maps corresponding to d
Point | A | R2 B | C | D | R3 E | F |
---|---|---|---|---|---|---|
Mg (wt%) | 84.43 | 82.85 | 84.32 | 87.49 | 83.97 | 87.00 |
Gd (wt%) | 15.57 | 17.15 | 15.68 | 12.51 | 16.03 | 13.00 |
Table 3 Compositions of points marked in Fig. 12
Point | A | R2 B | C | D | R3 E | F |
---|---|---|---|---|---|---|
Mg (wt%) | 84.43 | 82.85 | 84.32 | 87.49 | 83.97 | 87.00 |
Gd (wt%) | 15.57 | 17.15 | 15.68 | 12.51 | 16.03 | 13.00 |
Fig. 15 (0001) pole figure of deformed grains in a R1, d R2 and g R3; (0001) pole figure of dynamic recrystaillized grains in b R1, e R2 and h R3; the basal pole titled angle statistical distribution of deformed and recrystallized grains in c R1, f R2 and i R3
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