Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (8): 1397-1406.DOI: 10.1007/s40195-021-01371-6

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Evolution of micro-pores in a single crystal nickel-based superalloy during 980 °C creep

Yufeng He1,2, Shaogang Wang3, Jian Shen1(), Dong Wang1, Yuzhang Lu1, Langhong Lou1, Jian Zhang1()   

  1. 1Superalloys Division, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China
    2School of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China
    3Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China
  • Received:2021-09-25 Revised:2021-10-17 Accepted:2021-10-22 Online:2022-02-25 Published:2022-02-25
  • Contact: Jian Shen,Jian Zhang
  • About author:Jian Zhang jianzhang@imr.ac.cn
    Jian Shen shenjian@imr.ac.cn;

Abstract:

The evolution of micro-pores in a single crystal nickel-based superalloy during creep at 980 °C/220 MPa was investigated by X-ray computed tomography. Time-dependent ex-situ 3D information including the number, volume fraction, distribution and morphology of micro-pores was analyzed. The results reveal that the significant formation and growth of micro-pores occur at the end of secondary/beginning of tertiary creep stage. The irregular large pores as well as high density pores located at strain concentration region are the major detrimental factors facilitating the creep damage. Creep failure is resulted from the connection of surface cracks induced by oxidation, and the internal cracks generated from growth and merging of micro-pores.

Key words: Single crystal superalloy, Creep damage, Micro-pore evolution, X-ray tomography