Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (1): 163-175.DOI: 10.1007/s40195-021-01299-x
Dong-Fu Song1,2, Yu-Liang Zhao3, Zhi Wang1, Yi-Wang Jia2, Dao-Xi Li1, Ya-Nan Fu4, Da-Tong Zhang1, Wei-Wen Zhang1()
Received:
2021-05-27
Revised:
2021-06-26
Accepted:
2021-06-28
Online:
2022-01-10
Published:
2021-08-19
Contact:
Wei-Wen Zhang
About author:
Wei-Wen Zhang, mewzhang@scut.edu.cnDong-Fu Song, Yu-Liang Zhao, Zhi Wang, Yi-Wang Jia, Dao-Xi Li, Ya-Nan Fu, Da-Tong Zhang, Wei-Wen Zhang. 3D Fe-Rich Phases Evolution and Its Effects on the Fracture Behavior of Al-7.0Si-1.2Fe Alloys by Mn Neutralization[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(1): 163-175.
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Fig. 1 a SRXCT experimental setup used at beamline BL13W1 in the SSRF, b sample holder, c slice overlay, d region selection, e thresholding, f reconstruction
Alloy | Number | Volume fraction (%) | Equivalent diameter (μm) | Sphericity | Mean curvature | Thickness (μm) | Connectivity |
---|---|---|---|---|---|---|---|
Mn00 | 1 | 7.99 | ≥ 266 | 0.03 | 0.09 ± 0.22 | 3.39 ± 2.12 | 0.99 |
Mn12 | 557 | 4.91 | 20.9 ± 12.9 | 0.50 ± 0.21 | 0.11 ± 0.23 | 7.71 ± 5.43 | 0.03 |
Mn16 | 846 | 5.13 | 15.2 ± 11.5 | 0.66 ± 0.17 | 0.06 ± 0.20 | 7.65 ± 6.42 | 0.06 |
Table 1 3D statistics of iron-rich phases with different Mn contents (0.5 mm?×?0.5 mm?×?0.5 mm)
Alloy | Number | Volume fraction (%) | Equivalent diameter (μm) | Sphericity | Mean curvature | Thickness (μm) | Connectivity |
---|---|---|---|---|---|---|---|
Mn00 | 1 | 7.99 | ≥ 266 | 0.03 | 0.09 ± 0.22 | 3.39 ± 2.12 | 0.99 |
Mn12 | 557 | 4.91 | 20.9 ± 12.9 | 0.50 ± 0.21 | 0.11 ± 0.23 | 7.71 ± 5.43 | 0.03 |
Mn16 | 846 | 5.13 | 15.2 ± 11.5 | 0.66 ± 0.17 | 0.06 ± 0.20 | 7.65 ± 6.42 | 0.06 |
Fig. 5 3D statistical distribution of Fe-rich phases in alloys with different Mn contents: a equivalent diameter, b sphericity, c surface thickness, d mean curvature
Fig. 7. 3D structure and surface thickness distribution of Fe-rich phases with typical morphologies: a platelet-like, b regular polyhedron, c low-branched polyhedron, d low-branched hollow polyhedron, e, f multibranched hollow polyhedron
Fig. 8 Mean curvature distribution of Fe-rich phases with typical morphologies: a platelet-like, b regular polyhedron; c low-branched polyhedron, d low-branched hollow polyhedron, e, f multibranched hollow polyhedron
Phase | Elastic modulus (GPa) | Hardness (GPa) |
---|---|---|
α-Al15(FeMn)3Si2 [ | 199 | 14.8 |
α-AlFeSi [ | 183.81 ± 8.64 | - |
β-Al5FeSi [ | 196 | 11.5 |
β-AlFeSi [ | 174.13 ± 6.81 | - |
Si [ | 185 | 13.3 |
Al [ | 92 | 2.1 |
Table 2 Elastic modulus and hardness of phases in Al-Si-Fe-Mn alloys
Phase | Elastic modulus (GPa) | Hardness (GPa) |
---|---|---|
α-Al15(FeMn)3Si2 [ | 199 | 14.8 |
α-AlFeSi [ | 183.81 ± 8.64 | - |
β-Al5FeSi [ | 196 | 11.5 |
β-AlFeSi [ | 174.13 ± 6.81 | - |
Si [ | 185 | 13.3 |
Al [ | 92 | 2.1 |
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