Acta Metallurgica Sinica (English Letters) ›› 2016, Vol. 29 ›› Issue (4): 344-352.DOI: 10.1007/s40195-016-0390-5
Special Issue: 2016年钢铁材料专辑
• Orginal Article • Previous Articles Next Articles
Jing Qin1, Ping Yang1(), Wei-Min Mao1,2, Feng Ye2, Li Liu2
Received:
2015-10-22
Revised:
2015-12-07
Online:
2016-03-05
Published:
2016-04-27
Jing Qin, Ping Yang, Wei-Min Mao, Feng Ye, Li Liu. Secondary Recrystallization Behaviors of Grain-Oriented 6.5 wt% Silicon Steel Sheets Produced by Rolling and Nitriding Processes[J]. Acta Metallurgica Sinica (English Letters), 2016, 29(4): 344-352.
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Fig. 1 Macrostructures, {200} pole figures (levels: 1, 2, 4, 6, 8), and ODFs (φ 2 = 45°, levels: 1, 2, 4, 6, 8, 10, 12, 16, 20, 25) of 0.3-mm-thick grain-oriented 6.5 wt% silicon steel sheets and the nitriding time of 30 s a, 60 sb, 90 s c
Thickness (mm) | Nitriding time (s) | Magnetic flux density (T) | Core loss (W/kg) | ||
---|---|---|---|---|---|
B 8 | B 50 | P1.0/50 | P 1.5/50 | ||
0.3 | 30 | 1.525 | 1.761 | 0.585 | 1.567 |
60 | 1.537 | 1.762 | 0.581 | 1.568 | |
90 | 1.555 | 1.775 | 0.603 | 1.502 | |
0.23 | 90 | 1.570 | 1.797 | 0.378 | 1.135 |
Table 1 Magnetic properties of grain-oriented 6.5 wt% silicon steel sheets at 50 Hz
Thickness (mm) | Nitriding time (s) | Magnetic flux density (T) | Core loss (W/kg) | ||
---|---|---|---|---|---|
B 8 | B 50 | P1.0/50 | P 1.5/50 | ||
0.3 | 30 | 1.525 | 1.761 | 0.585 | 1.567 |
60 | 1.537 | 1.762 | 0.581 | 1.568 | |
90 | 1.555 | 1.775 | 0.603 | 1.502 | |
0.23 | 90 | 1.570 | 1.797 | 0.378 | 1.135 |
Fig. 3 Orientation images and ODFs (φ 2 = 0°, 45°; levels: 1, 2, 3, 4, 5) of the samples, which are nitrided for 30 sa, 60 s b, and 90 s c and their area fractions of main texture components d
Fig. 4 Local orientation images, {200} pole figures, and ODFs (levels: 1, 2, 4, 8, 10, 20, 40, 80) of the samples, which are nitrided for 60 s and extracted at 850 °C a, 875 °C b, 900 °C c, 925 °C d, 950 °C e, 975 °C f, 1000 °C, g 1050 °C h, and 1075 °C i during the secondary recrystallization annealing
Temperature (°C) | {112}?110? | {112}?241? | {111}?110? | {111}?112? | {210}?001? | {100}?011? | {100}?001? | {110}?116? | {110}?001? |
---|---|---|---|---|---|---|---|---|---|
850 | 0.5 | 25.8 | 0.2 | 6.8 | 7.0 | 2.3 | 6.5 | 5.5 | 3.5 |
875 | 4.0 | 12.0 | 1.0 | 5.2 | 16.9 | 2.5 | 6.5 | 6.5 | 2.2 |
900 | 3.5 | 16.5 | 2.5 | 6.0 | 7.7 | 0.2 | 5.4 | 5.0 | 4.3 |
925 | 5.3 | 15.2 | 3.7 | 4.1 | 9.2 | 1.0 | 4.4 | 17 | 4.2 |
950 | 0 | 0 | 0 | 0 | 32.3 | 0 | 0 | 53.1 | 0 |
Table 2 Area fractions of main texture components in Fig. 4 (%)
Temperature (°C) | {112}?110? | {112}?241? | {111}?110? | {111}?112? | {210}?001? | {100}?011? | {100}?001? | {110}?116? | {110}?001? |
---|---|---|---|---|---|---|---|---|---|
850 | 0.5 | 25.8 | 0.2 | 6.8 | 7.0 | 2.3 | 6.5 | 5.5 | 3.5 |
875 | 4.0 | 12.0 | 1.0 | 5.2 | 16.9 | 2.5 | 6.5 | 6.5 | 2.2 |
900 | 3.5 | 16.5 | 2.5 | 6.0 | 7.7 | 0.2 | 5.4 | 5.0 | 4.3 |
925 | 5.3 | 15.2 | 3.7 | 4.1 | 9.2 | 1.0 | 4.4 | 17 | 4.2 |
950 | 0 | 0 | 0 | 0 | 32.3 | 0 | 0 | 53.1 | 0 |
Fig. 6 Distribution of the precipitates at 875 °C a, 900 °C b, and 925 °C c in the surface and the central layer of samples nitrided 60 s and EDS analysis of the precipitates d
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