Acta Metallurgica Sinica (English Letters) ›› 2021, Vol. 34 ›› Issue (2): 248-264.DOI: 10.1007/s40195-020-01120-1
Previous Articles Next Articles
Ce Zheng1,2, Shuai-Feng Chen1,3, Rui-Xue Wang1, Shi-Hong Zhang1, Ming Cheng1()
Received:
2020-02-18
Revised:
2020-05-27
Accepted:
2020-05-31
Online:
2021-02-10
Published:
2021-02-09
Contact:
Ming Cheng
Ce Zheng, Shuai-Feng Chen, Rui-Xue Wang, Shi-Hong Zhang, Ming Cheng. Effect of Hydrostatic Pressure on LPSO Kinking and Microstructure Evolution of Mg-11Gd-4Y-2Zn-0.5Zr Alloy[J]. Acta Metallurgica Sinica (English Letters), 2021, 34(2): 248-264.
Add to citation manager EndNote|Ris|BibTeX
Fig. 1 Distribution of effective plastic strain for a normal-compression, b can-compression at final state; evolution of c effective plastic strain, d stress triaxiality for the selected center element
Fig. 2 EBSD results of as-homogenized GWZK114 alloy a orientation imaging microscopy (OIM); b statistical distribution of grain size; c (0001) pole figure (PF); d backscattered electron (BSE) image; TEM results of e intragranular needle-like phase; f intergranular bulk phase; g-i EDS results of points A, B, and C in Fig. 2d. The CD and RD indicate the compression and radial directions, respectively
Fig. 4 OM microstructure of as-compressed GWZK 114 alloy under two hydrostatic pressures for different deformation conditions. The DRX area fractions are also presented and calculated as fDRX = SDRX/(SAll - SInter) with SDRX and SInter being the areas of DRX grains and intergranular phases, respectively
Fig. 5 SEM images of the kink behavior of LPSO phases under different conditions; 14H and 18R-LPSO phases were marked by red and yellow lines, respectively, and the curved ones represent the kinking of LPSO phase
Fig. 6 Kinking behavior of LPSO phases in normal and can-compressed samples: a kink angle; b kink times; c relative width ratio of kink band (d/L). d schematic of width, kink times and angle for kink band. For a certain deformation case in Fig. 6a-c, at least ten measures are taken for these statistics
Fig. 8 Kernel average misorientation (KAM) maps of samples under normal-compression of a 350 °C, d 450 °C; can-compression of b 350 °C, e 450 °C; distribution of local misorientation of KAM under c 350 °C, f 450 °C
Contents | Normal-compression | Can-compression | ||
---|---|---|---|---|
350 °C | 450 °C | 350 °C | 450 °C | |
θlocal (°) | 1.19 | 0.69 | 1.41 | 0.79 |
ρGND (/m2, × 1014) | 0.96 | 0.33 | 1.36 | 0.43 |
Table 1 Average local misorientation and calculated dislocation density under different conditions
Contents | Normal-compression | Can-compression | ||
---|---|---|---|---|
350 °C | 450 °C | 350 °C | 450 °C | |
θlocal (°) | 1.19 | 0.69 | 1.41 | 0.79 |
ρGND (/m2, × 1014) | 0.96 | 0.33 | 1.36 | 0.43 |
Fig. 10 DRX behavior of grain G1 in Fig. 7c: a orientation imaging microscopy (OIM); b line profile of misorientation angle along the lines A-B in a; c Schmid factors of basal 〈a〉, prismatic 〈a〉 and pyramidal 〈c + a〉 slip systems for grain G1 under normal-compression condition. (Basal 〈a〉: $\left\{ {0001} \right\}\left\langle {11\bar{2}0} \right\rangle$; prismatic 〈a〉: $\left\{ {10\bar{1}0} \right\}\left\langle {11\bar{2}0} \right\rangle$; pyramidal 〈c + a〉: $\left\{ {11\bar{2}2} \right\}\left\langle {11\bar{2}3} \right\rangle$)
Fig. 11 DRX behavior of grain G3 in Fig. 7d: a orientation imaging microscopy (OIM); b line profile of misorientation angle along the lines E-F in a; c the Schmid factors of basal 〈a〉, prismatic 〈a〉 and pyramidal 〈c + a〉 slip systems for grain G3 under can-compression condition
Fig. 12 DRX behavior of grain G2 in Fig. 7c: a orientation imaging microscopy (OIM); b band contract figure; c line profile of misorientation angle along the lines C-D in a; d the Schmid factors of basal 〈a〉, prismatic 〈a〉 and pyramidal 〈c + a〉 slip systems for grain G2 under normal-compression condition
Fig. 13 DRX behavior of grain G4 in Fig. 7d: a orientation imaging microscopy (OIM); b band contract figure c line profile of misorientation angle along the lines G-H in a, d Schmid factors of basal 〈a〉, prismatic 〈a〉 and pyramidal 〈c + a〉 slip systems for grain G4 under can-compression condition
Fig. 14 Schematic of kink band formation under different loading conditions: a compression with a small inclined α angle of CD from 14H-LPSO phase’s basal planes; b compression with a high inclined α angle of CD from 14H-LPSO phase’s basal planes
[1] | Z. Zeng, N. Stanford, C.H.J. Davies, J.F. Nie, N. Birbilis, Int. Mater. Rev. 64, 27(2019) |
[2] |
C. Xu, T. Nakata, X. Qiao, M.Y. Zheng, K. Wu, S. Kamado, Sci. Rep. 7, 40846(2017)
URL PMID |
[3] | S.J. Meng, H. Yu, S.D. Fan, Q.Z. Li, S.H. Park, J.S. Suh, Y.M. Kim, X.L. Nan, M.Z. Bian, F.X. Yin, W.M. Zhao, B.S. You, K.S. Shin, Acta Metall. Sin. (Engl. Lett.) 32, 145(2019) |
[4] | B.L. Mordike, T. Ebert, Mater. Sci. Eng. A 302, 37 (2001) |
[5] | L.Z. Liu, F.S. Pan, X.H. Chen, Y.D. Huang, B. Song, H. Yang, N. Hort, Vacuum 155, 445 (2018) |
[6] | B.N. Du, Z.Y. Hu, L.Y. Sheng, D.K. Xu, Y.F. Zheng, T.F. Xi, Acta Metall. Sin. (Engl. Lett.) 31, 351(2018) |
[7] | J. Yang, J. Peng, M. Li, E.A. Nyberg, F.S. Pan, Acta Metall. Sin. (Engl. Lett.) 30, 53(2017) |
[8] | B. Pourbahari, H. Mirzadeh, M. Emamy, Mater. Sci. Eng. A 680, 39 (2017) |
[9] | Q.Z. Liu, X.F. Ding, Y.P. Liu, X.J. Wei, J. Alloys Compd. 690, 961(2017) |
[10] | F.Q. Bu, Q. Yang, K. Guan, X. Qiu, D.P. Zhang, W. Sun, T. Zheng, X.P. Cui, S.C. Sun, Z.M. Tang, X.J. Liu, J. Meng, J. Alloys Compd. 688, 1241(2016) |
[11] | M.X. Wang, H. Zhou, L. Wang, J. Rare Earth 25, 233 (2007) |
[12] | F. Zhong, H.J. Wu, Y.L. Jiao, R.Z. Wu, J.H. Zhang, L.G. Hou, M.L. Zhang, J. Mater. Sci. Technol. 39, 124(2020) |
[13] | X.H. Shao, Z.Q. Yang, X.L. Ma, Acta Mater. 58, 4760(2010) |
[14] | H. Gao, K. Ikeda, T. Morikawa, K. Higashida, H. Nakashima, Mater. Lett. 146, 30(2015) |
[15] | K. Máthis, G. Farkas, G. Garcés, J. Gubicza, Mater. Lett. 190, 86(2017) |
[16] | R. Chen, S. Sandlöbes, X.Q. Zeng, D.J. Li, K.K. Sandra, D. Raabe, Mater. Sci. Eng. A 682, 354 (2017) |
[17] | T. Homma, N. Kunito, S. Kamado, Scr. Mater. 61, 644(2009) |
[18] | C. Xu, M.Y. Zheng, S. Xu, K. Wu, E.D. Wang, G.H. Fan, S. Kamado, Mater. Sci. Eng. A 643, 137 (2015) |
[19] | L. Li, Y. Wang, C.C. Zhang, T. Wang, H. Lv, W.B. Yu, Vacuum 173, 109157 (2020) |
[20] |
C. Xu, S.W. Xu, M.Y. Zheng, K. Wu, E.D. Wang, S. Kamado, G.J. Wang, X.Y. Lv, J. Alloys Compd. 524, 46(2012)
DOI URL |
[21] | G.S. Zhang, Z.M. Zhang, Y. Du, Z.M. Yan, X. Che, Materials 11, 2092 ( 2018) |
[22] |
B. Li, B.G. Teng, D.G. Luo, Acta Metall. Sin. (Engl. Lett.) 31, 1009(2018)
DOI URL |
[23] | F.P. Bullen, F. Henderson, M.M. Hutchison, H.L. Wain, Philos. Mag. 9, 285(1964) |
[24] | F.P. Bullen, F. Henderson, H.L. Wain, M.S. Paterson, Philos. Mag. 101, 803(1964) |
[25] |
J.J. Lewandowski, P. Lowhaphandu, Int. Mater. Rev. 43, 145(1998)
DOI URL |
[26] | I.E. French, P.F. Weinrich, Metall. Trans. A 6, 785 (1975) |
[27] | M.J. Zehetbauer, H.P. Stüwe, A. Vorhauer, E. Schafler, J. Kohout, Adv. Eng. Mater. 5, 330(2003) |
[28] | H.X. Zhang, S.F. Chen, M. Cheng, C. Zheng, S.H. Zhang, Acta. Metall. Sin. (Engl. Lett.) 32, 1122(2019) |
[29] | D. Pradhan, G.S. Mahobia, K. Chattopadhyay, D.C. Fernando, N. Paulose, S.N.N. Babu, V. Singh, Mater. Res. Express 6, 0965a6 (2019) |
[30] | Y. Lou, J.W. Yoon, H. Huh, Int. J. Plast. 54, 56(2014) |
[31] | J.B. Shao, Z.Y. Chen, C. Tao, C.M. Liu, Metall. Mater. Trans. A 51, 1911 (2020) |
[32] | X.J. Zhou, C.M. Liu, Y.H. Gao, S.N. Jiang, X.Z. Han, Z.Y. Cheng, Metall. Mater. Trans. A 48, 3060 (2017) |
[33] | A.P. Zhilyaev, S.N. Sergeev, T.G. Langdon, J. Mater. Res. Technol. 3, 338(2014) |
[34] | K. Hagihara, M. Yamasaki, M. Honnami, H. Izuno, M. Tane, T. Nakano, Y. Kawamura, Philos. Mag. 95, 132(2015) |
[35] | M.R. Barnett, Metall. Mater. Trans. A 34, 1799 (2003) |
[36] | J. Jiang, T.B. Britton, A.J. Wilkinson, Acta Mater. 94, 193(2015) |
[37] | S.S.A. Shah, M.G. Jiang, D. Wu, U. Wasi, R.S. Chen, Acta Metall. Sin. (Engl. Lett.) 31, 923(2018) |
[38] | S. Biswas, B. Beausir, L.S. Toth, S. Suwas, Acta Mater. 61, 5263(2013) |
[39] | A. Galiyev, R. Kaibyshev, G. Gottstein, Acta Mater. 49, 1199(2001) |
[40] | A. Couret, D. Caillard, Acta Metall. 33, 1447(1985) |
[41] | W. Püschl, G. Schoeck, H.O.K. Kirchner, Philos. Mag. 56, 553(1987) |
[42] | M.G. Jiang, C. Xu, G.H. Fan, T. Nakata, C.S. Lao, R.S. Chen, S. Kamado, E.H. Han, B.H. Lu, Acta Mater. 157, 53(2018) |
[43] | T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, J.J. Jonas, Prog. Mater. Sci. 60, 130(2014) |
[44] | S.F. Chen, H.W. Song, S.H. Zhang, M. Cheng, C. Zheng, M.G. Lee, Scr. Mater. 167, 51(2019) |
[45] | S.F. Chen, H.W. Song, S.H. Zhang, M. Cheng, M.G. Lee, J. Alloys Compd. 805, 138(2019) |
[46] | C.D. Barrett, A. Imandoust, A.L. Oppedal, K. Inal, M.A. Tschopp, H.E. Kadiri, Acta Mater. 128, 270(2017) |
[47] | Y.N. Wang, J.C. Huang, Mater. Chem. Phys. 81, 11(2003) |
[1] | Baojie Wang, Daokui Xu, Tianyu Zhao, Liyuan Sheng. Effect of CaCl2 and NaHCO3 in Physiological Saline Solution on the Corrosion Behavior of an As-Extruded Mg-Zn-Y-Nd alloy [J]. Acta Metallurgica Sinica (English Letters), 2021, 34(2): 239-247. |
[2] | Meng Yan, Cong Wang, Tianjiao Luo, Yingju Li, Xiaohui Feng, Qiuyan Huang, Yuansheng Yang. Effect of Pulsed Magnetic Field on the Residual Stress of Rolled Magnium Alloy AZ31 Sheet [J]. Acta Metallurgica Sinica (English Letters), 2021, 34(1): 45-53. |
[3] | Jiaqi Hu, Qite Li, Hong Gao. Influence of Twinning Texture on the Corrosion Fatigue Behavior of Extruded Magnesium Alloys [J]. Acta Metallurgica Sinica (English Letters), 2021, 34(1): 65-76. |
[4] | Zheng-Zheng Yin, Zhao-Qi Zhang, Xiu-Juan Tian, Zhen-Lin Wang, Rong-Chang Zeng. Corrosion Resistance and Durability of Superhydrophobic Coating on AZ31 Mg Alloy via One-Step Electrodeposition [J]. Acta Metallurgica Sinica (English Letters), 2021, 34(1): 25-38. |
[5] | Lin-Yue Jia, Wen-Bo Du, Jin-Long Fu, Zhao-Hui Wang, Ke Liu, Shu-Bo Li, Xian Du. Obtaining Ultra-High Strength and Ductility in a Mg-Gd-Er-Zn-Zr Alloy via Extrusion, Pre-deformation and Two-Stage Aging [J]. Acta Metallurgica Sinica (English Letters), 2021, 34(1): 39-44. |
[6] | Li-Sha Wang, Jing-Hua Jiang, Bassiouny Saleh, Qiu-Yuan Xie, Qiong Xu, Huan Liu, Ai-Bin Ma. Controlling Corrosion Resistance of a Biodegradable Mg-Y-Zn Alloy with LPSO Phases via Multi-pass ECAP Process [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(9): 1180-1190. |
[7] | Fenghua Wang, Peng Su, Linxin Qin, Shuai Dong, Yunliang Li, Jie Dong. Microstructure and Mechanical Properties of Mg-3Al-Zn Magnesium Alloy Sheet by Hot Shear Spinning [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(9): 1226-1234. |
[8] | Kai-Bo Nie, Zhi-Hao Zhu, Paul Munroe, Kun-Kun Deng, Jun-Gang Han. Microstructure, Tensile Properties and Work Hardening Behavior of an Extruded Mg-Zn-Ca-Mn Magnesium Alloy [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(7): 922-936. |
[9] | Yang Shao, Rong-Chang Zeng, Shuo-Qi Li, Lan-Yue Cui, Yu-Hong Zou, Shao-Kang Guan, Yu-Feng Zheng. Advance in Antibacterial Magnesium Alloys and Surface Coatings on Magnesium Alloys: A Review [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(5): 615-629. |
[10] | Kwang-Su Kim, Lin-Xiu Du, Hyo-sung Choe, Tae-Hyong Lee, Gyong-Chol Lee. Influence of Vanadium Content on Hot Deformation Behavior of Low-Carbon Boron Microalloyed Steel [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(5): 705-715. |
[11] | Longlong Zhang, Yatong Zhang, Jinshan Zhang, Rui Zhao, Jiaxin Zhang, Chunxiang Xu. Effect of Alloyed Mo on Mechanical Properties, Biocorrosion and Cytocompatibility of As-Cast Mg-Zn-Y-Mn Alloys [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(4): 500-513. |
[12] | Yan Dai, Xian-Hua Chen, Tao Yan, Ai-Tao Tang, Di Zhao, Zhu Luo, Chun-Quan Liu, Ren-Ju Cheng, Fu-Sheng Pan. Improved Corrosion Resistance in AZ61 Magnesium Alloys Induced by Impurity Reduction [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(2): 225-232. |
[13] | A. Shah S., D. Wu, Chen R. S., Song G. S.. Temperature Effects on the Microstructures of Mg-Gd-Y Alloy Processed by Multi-direction Impact Forging [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(2): 243-251. |
[14] | Pei Li, Danhui Hou, En-Hou Han, Rongshi Chen, Zhiwei Shan. Solidification of Mg-Zn-Zr Alloys: Grain Growth Restriction, Dendrite Coherency and Grain Size [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(11): 1477-1486. |
[15] | Yabo Zhang, Huiling Yang, Shaoqian Lei, Shijie Zhu, Jianfeng Wang, Yufeng Sun, Shaokang Guan. Preparation of Biodegradable Mg/β-TCP Biofunctional Gradient Materials by Friction Stir Processing and Pulse Reverse Current Electrodeposition [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(1): 103-114. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||