Acta Metallurgica Sinica (English Letters) ›› 2025, Vol. 38 ›› Issue (10): 1719-1734.DOI: 10.1007/s40195-025-01900-7
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Lihua Zhu, Bing Wei(
), Kaiqi Wang, Changjie Zhou, Hongjun Ji(
)
Received:2025-01-20
Revised:2025-03-25
Accepted:2025-04-06
Online:2025-06-30
Published:2025-06-30
Contact:
Bing Wei, Hongjun Ji
Lihua Zhu, Bing Wei, Kaiqi Wang, Changjie Zhou, Hongjun Ji. Optimizing Selective Laser Melting of a High-Alloyed Ni-Based Superalloy: Achieving Crack-Free Fabrication with Enhanced Microstructure and Mechanical Properties[J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1719-1734.
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| Co | Cr | Al | Ti | Mo | W | Nb | Ta | C | B | Zr | Ni |
|---|---|---|---|---|---|---|---|---|---|---|---|
| 25.0 | 13.0 | 3.9 | 2.5 | 3.5 | 3.9 | 1.0 | 1.2 | 0.03 | 0.005 | 0.005 | Bal. |
Table 1 Chemical composition of the powders used in the present investigation (wt%)
| Co | Cr | Al | Ti | Mo | W | Nb | Ta | C | B | Zr | Ni |
|---|---|---|---|---|---|---|---|---|---|---|---|
| 25.0 | 13.0 | 3.9 | 2.5 | 3.5 | 3.9 | 1.0 | 1.2 | 0.03 | 0.005 | 0.005 | Bal. |
Fig. 1 Morphology characterization of novel Ni-based superalloy powder particles: a microstructure morphology of powder particle, b distribution of powder particle size, c element distribution of powder particle
Fig. 2 Schematic diagram of laser power, scanning speed, and scanning strategy: a parameter optimization and the cube specimens of size 10 mm × 10 mm × 15 mm obtained from SLM experiment, b scanning strategy of SLM
| Parameters | Value |
|---|---|
| Laser power, p (W) | 200, 225, 250, 275 |
| Scanning speed, v (mm/s) | 600, 800, 1000, 1200 |
| Hatch spacing, h (mm) | 0.11 |
| Layer thickness, t (mm) | 0.04 |
| Laser beam spot size, d (mm) | 0.08 |
| Rotation between layers (°) | 67 |
| Substrate preheating temperature (℃) | 200 |
| Volume energy density, η (J/mm3) | 37.9-104.2 |
Table 2 Key processing parameters used for the SLM of new Ni-based superalloy
| Parameters | Value |
|---|---|
| Laser power, p (W) | 200, 225, 250, 275 |
| Scanning speed, v (mm/s) | 600, 800, 1000, 1200 |
| Hatch spacing, h (mm) | 0.11 |
| Layer thickness, t (mm) | 0.04 |
| Laser beam spot size, d (mm) | 0.08 |
| Rotation between layers (°) | 67 |
| Substrate preheating temperature (℃) | 200 |
| Volume energy density, η (J/mm3) | 37.9-104.2 |
Fig. 4 Evolution of relative density with different laser parameters: a relationship between power, scanning rate, and relative density, b relationship between energy density and relative density
Fig. 5 Metallographic structure and SEM images of the XZ plane of as-printed samples at different energy densities: a, b 37.9 J/mm3, c, d 51.1 J/mm3, e, f 71.0 J/mm3, and g, h 104.2 J/mm3
Fig. 7 Inverse pole figures (IPFs), band contrast (BC), average grain size distribution, and pole figures (PF) at different energy densities: a, e, i, m 37.9 J/mm3, b, f, j, n 51.1 J/mm3, c, g, k, o 71.0 J/mm3, d, h, l, p 104.2 J/mm3
Fig. 8 TEM observations from the XY plane in the SLM samples with η = 71.0 J/mm3: a, b the bright field TEM micrograph in the XY plane, c the selected area electron diffraction (SAED) pattern, d high-angle annular dark-field scanning transmission electron microscopy image and the relevant EDS mapping
Fig. 9 Tensile performance of printed alloys at varying energy densities: a engineering stress-strain curves, b comparison of tensile properties [44,45,46,47,48,49,50,51,52,53,54,55,56,57,58]
Fig. 10 Tensile performance of printed alloys with an energy density of 51.1 J/mm3 at 750 °C: a engineering stress-strain curves, b nanoscale γ′ phase particles, c comparison of tensile properties [48,49,50,56,59,60]
Fig. 11 SEM fracture images of printed alloys at varying energy densities: a, e, i 37.9 J/mm3, b, f, j 51.1 J/mm3, c, g, k 71.0 J/mm3, d, h, l 104.2 J/mm3
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