Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (9): 1424-1438.DOI: 10.1007/s40195-022-01419-1
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Junwei Sha1(), Meixian Li1, Lizhuang Yang1, Xudong Rong1, Bowen Pu1, Dongdong Zhao1, Simi Sui1, Xiang Zhang1, Chunnian He1,2,3, Jianglin Lan4, Naiqin Zhao1,2,3
Received:
2022-03-07
Revised:
2022-04-01
Accepted:
2022-04-01
Online:
2022-09-10
Published:
2022-05-25
Contact:
Junwei Sha
About author:
Junwei Sha, shajw@tju.edu.cnJunwei Sha, Meixian Li, Lizhuang Yang, Xudong Rong, Bowen Pu, Dongdong Zhao, Simi Sui, Xiang Zhang, Chunnian He, Jianglin Lan, Naiqin Zhao. Si-Assisted Solidification Path and Microstructure Control of 7075 Aluminum Alloy with Improved Mechanical Properties by Selective Laser Melting[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(9): 1424-1438.
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Laser power (W) | Scanning velocity (mm/s) | Layer thickness (mm) | Hatch space (mm) |
---|---|---|---|
150, 270, 300, 330 | 200, 400, 600, 800, 1000, 1200, 1400, 1600, 1800 | 0.03 | 0.1 |
Table 1 Specific SLM parameters used in this work
Laser power (W) | Scanning velocity (mm/s) | Layer thickness (mm) | Hatch space (mm) |
---|---|---|---|
150, 270, 300, 330 | 200, 400, 600, 800, 1000, 1200, 1400, 1600, 1800 | 0.03 | 0.1 |
Fig. 1 a Temperature vs. (fs)1/2 curves of Al7075 and Al7075-5Si alloy; solidification paths of b Al7075, c Al7075-5Si alloys simulated by using Scheil-Gulliver model in Thermo-Calc software
Fig. 2 SEM image and elements distribution of Al7075-5Si powders detected by using EDS mapping: a SEM image of Al7075-5Si powders, b Al, c Si, d Mg, e Cu, f Zn
Fig. 4 a Vickers hardness testing of Al7075-5Si cubes with different laser energy densities at the different positions along the same direction, b engineering stress-strain curves of Al7075-5Si alloy with different laser energy densities after SLM printing
Laser energy density (J/mm3) | YS (MPa) | UTS (MPa) | Elongation (%) | Hardness (HV0.2) |
---|---|---|---|---|
62 | 338 ± 4 | 362 ± 1 | 0.4 ± 0.1 | 160 ± 4 |
112.5 | 291 ± 8 | 486 ± 3 | 6.4 ± 0.4 | 162 ± 2 |
138 | 237 ± 16 | 418 ± 11 | 5.2 ± 1.2 | 159 ± 3 |
225 | 221 ± 15 | 373 ± 1 | 4.7 ± 0.5 | 152 ± 4 |
Table 2 Mechanical properties of SLM-processed Al7075-5Si alloy at different laser energy densities
Laser energy density (J/mm3) | YS (MPa) | UTS (MPa) | Elongation (%) | Hardness (HV0.2) |
---|---|---|---|---|
62 | 338 ± 4 | 362 ± 1 | 0.4 ± 0.1 | 160 ± 4 |
112.5 | 291 ± 8 | 486 ± 3 | 6.4 ± 0.4 | 162 ± 2 |
138 | 237 ± 16 | 418 ± 11 | 5.2 ± 1.2 | 159 ± 3 |
225 | 221 ± 15 | 373 ± 1 | 4.7 ± 0.5 | 152 ± 4 |
Fig. 5 a Vickers hardness testing of Al7075 and Al7075-5Si cubes under the laser energy density of 112.5 J/mm3 at the different positions along the same direction; b engineering stress-strain curves of SLM-processed Al7075 and Al7075-5Si alloy under the laser energy density of 112.5 J/mm3, c mechanical properties comparison of SLM-processed Al alloys from different literature [10,17,23,24,25,37,38,39,40,41,42,43]
Materials | YS (MPa) | UTS (MPa) | Elongation (%) | Hardness (HV0.2) |
---|---|---|---|---|
Al7075-5Si | 291 ± 8 | 486 ± 3 | 6.4 ± 0.4 | 162 ± 2 |
Al7075 | NA | 41 ± 2 | NA | 111 ± 8 |
Table 3 Mechanical properties of SLM-processed Al7075 and Al7075-5Si
Materials | YS (MPa) | UTS (MPa) | Elongation (%) | Hardness (HV0.2) |
---|---|---|---|---|
Al7075-5Si | 291 ± 8 | 486 ± 3 | 6.4 ± 0.4 | 162 ± 2 |
Al7075 | NA | 41 ± 2 | NA | 111 ± 8 |
Fig. 6 SEM images of fracture surfaces of a, b Al7075 alloy and c, d Al7075-5Si alloy after SLM printing, the inset in d is the enlargement of dimple in d
Fig. 9 EBSD analysis results of SLM-processed samples in the building direction. Inverse pole figure maps of a Al7075 and b Al7075-5Si; d, e distribution of sub-structural grains (in yellow) and recrystallized grains (in blue) of a, b, respectively; g, h {100}, {110} and {111} pole figures corresponding to the textures intensity of a, b, respectively; c and f grain size distribution and XRD patterns of SLM-processed Al7075 and Al7075-5Si samples, respectively
Fig. 10 a Scanning transmission electron microscopy (STEM) bright-field image of Al7075-5Si, showing the precipitated phases at the grain boundaries. The green arrows point the eutectic Si, and the purple arrows are the Mg2Si phase; b-f EDS elements distribution analysis results: b Al, c Zn, d Mg, e Cu, f Si; g, h TEM images and the corresponding selected area electron diffraction (SAED) patterns of Al7075-5Si, showing the phase composition in the marked zones A and B
Fig. 11 a STEM bright-field image of the precipitates in Al7075-5Si, and b EDS elemental line distribution analysis result in the marked arrow direction in a
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