Influence of Nb Content on Microstructure and Mechanical Properties of a 7%Ni Steel

doi:10.1007/s40195-018-0743-3

Abstract

Abstract:

The influence of Nb content on the microstructure and cryogenic mechanical properties of a 7%Ni steel was investigated within the Nb content range from 0 to 0.05%. The microstructure was characterized by optical microscope, scanning electron microscope, transmission electron microscopy and X-ray diffraction, and the low-temperature mechanical property tests were conducted. The Nb addition can effectively refine the prior austenite grains and microstructure of the steel. Fine niobium precipitates with a diameter of about 10-50 nm were observed. They tend to be spherical and locate mainly in the vicinity of grain boundaries. Although there are considerable amounts of reversed austenite forming at grain boundaries in the specimen containing the highest Nb content, no Nb element was detected in such reversed austenite, which implies that Nb element did not affect the formation of the reversed austenite directly. Mechanical test results suggest that the strength of the 7%Ni steel is not simply in relation to the prior austenite grain size, but also depends on the amount of reversed austenite. On the other hand, the grain refinement, enhanced with increasing Nb content, has a good effect on cryogenic toughness.

Key words: 7%Ni steel, Nb content, Niobium precipitate, Reversed austenite, Cryogenic mechanical properties

Hong-Wei Cao, Xing-Hong Luo, Guo-Feng Zhan, Shi Liu. Influence of Nb Content on Microstructure and Mechanical Properties of a 7%Ni Steel[J]. Acta Metallurgica Sinica (English Letters), 2018, 31(9): 975-982.

Figures/Tables 11

Fig. 1 Scheme of heat treatment.

Fig. 2 OM a, c, e and SEM b, d, f images of specimens containing Nb contents of 0% a, b, 0.025% c, d, 0.05% e, f.

Fig. 3 Effect of Nb content on grain size of prior austenite.

Fig. 4 Morphologies of fine precipitates in Nb-microalloyed specimens: a 0.025%Nb; b 0.05%Nb.

Fig. 5 Pseudo-binary phase diagram of Nb-7%Ni steel.

Fig. 6 XRD patterns of specimens after heat treatment: a 0%Nb; b 0.025%Nb; c 0.05%Nb.

Fig. 7 Backscattered electron images of specimens containing different Nb contents: a 0%Nb; b 0.025%Nb; c 0.05% Nb.

Fig. 8 Morphologies of reversed austenite in specimens containing different Nb contents: a 0%Nb; b 0.025%Nb; c 0.05%Nb.

Fig. 9 Cryogenic tensile properties of specimens as a function of Nb content at -196 °C.

Fig. 10 Cryogenic toughness (Akv) of specimens as a function of Nb content at - 192 °C.

Fig. 11 Fracture morphologies of impact specimens containing different Nb contents: a 0%Nb; b 0.025%Nb; c 0.05%Nb.

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