Acta Metallurgica Sinica (English Letters) ›› 2024, Vol. 37 ›› Issue (8): 1411-1420.DOI: 10.1007/s40195-024-01711-2
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J. X. Cai1,4, B. M. Shi1,2, N. Li3, Y. Liu1, Z. G. Zhang4, Y. N. Zan1,2(
), Q. Z. Wang1,2, B. L. Xiao1, Z. Y. Ma1,2
Received:2024-01-10
Revised:2024-02-06
Accepted:2024-02-10
Online:2024-08-10
Published:2024-07-02
Contact:
Y. N. Zan, ynzan15b@imr.ac.cn
J. X. Cai, B. M. Shi, N. Li, Y. Liu, Z. G. Zhang, Y. N. Zan, Q. Z. Wang, B. L. Xiao, Z. Y. Ma. Effect of Al2O3 on the Mechanical Properties of (B4C + Al2O3)/Al Neutron Absorbing Materials[J]. Acta Metallurgica Sinica (English Letters), 2024, 37(8): 1411-1420.
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Fig. 1 SEM images of Al powders with average diameter of a 1.4 μm, b 2.3 μm, c 4.6 μm and d 7.0 μm, and the size distribution of e 1.4 μm, f 2.3 μm, g 4.6 μm and h 7.0 μm Al powders
| Diameter of Al powders (μm) | As-pressed composites | As-extruded composites |
|---|---|---|
| 1.4 | AP 1.4 | AE 1.4 |
| 2.3 | AP 2.3 | AE 2.3 |
| 4.6 | AP 4.6 | AE 4.6 |
| 7.0 | AP 7.0 | AE 7.0 |
Table 1 Designations of the composites with different Al2O3 contents
| Diameter of Al powders (μm) | As-pressed composites | As-extruded composites |
|---|---|---|
| 1.4 | AP 1.4 | AE 1.4 |
| 2.3 | AP 2.3 | AE 2.3 |
| 4.6 | AP 4.6 | AE 4.6 |
| 7.0 | AP 7.0 | AE 7.0 |
Fig. 3 STEM-BF images of a AP 1.4 and d AP 2.3, and the distribution of elements of b, c AP 1.4 and e, f AP 2.3; yellow arrows denote the original Al powder boundaries, and red arrows denote the GBs formed in the hot-pressing process
Fig. 4 a STEM-BF image and the element distribution of b Al, c O, d B, e C of AP 7.0; yellow arrows denote the original Al powder boundaries, and red arrows denote the GBs formed in the hot-pressing process
Fig. 5 TEM images of as-pressed (B4C + Al2O3)/Al composites: a AP 1.4, b AP 2.3, c AP 4.6 and d AP 7.0; the insets show Al2O3 with higher magnification
| Sample | RT | 350 °C | ||||
|---|---|---|---|---|---|---|
| YS (MPa) | UTS (MPa) | El (%) | YS (MPa) | UTS (MPa) | El (%) | |
| AE 1.4 | 219 | 259 | 6.3 | 121 | 127 | 5 |
| AE 2.3 | 202 | 234 | 9.8 | 105 | 110 | 12 |
| AE 4.6 | 165 | 192 | 13.8 | 90 | 95 | 13.2 |
| AE 7.0 | 145 | 167 | 16.7 | 74 | 78 | 23.2 |
Table 2 Mechanical properties of the as-extruded (B4C + Al2O3)/Al composites at RT and 350 °C
| Sample | RT | 350 °C | ||||
|---|---|---|---|---|---|---|
| YS (MPa) | UTS (MPa) | El (%) | YS (MPa) | UTS (MPa) | El (%) | |
| AE 1.4 | 219 | 259 | 6.3 | 121 | 127 | 5 |
| AE 2.3 | 202 | 234 | 9.8 | 105 | 110 | 12 |
| AE 4.6 | 165 | 192 | 13.8 | 90 | 95 | 13.2 |
| AE 7.0 | 145 | 167 | 16.7 | 74 | 78 | 23.2 |
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