Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (12): 2089-2100.DOI: 10.1007/s40195-022-01440-4
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Xinlei Zhou1,2, Bin Wang3, Tianyi Zeng1,2, Wei Yan2, Junhua Luan4, Wei Wang2(), Ke Yang2, Zengbao Jiao5
Received:
2022-04-12
Revised:
2022-05-13
Accepted:
2022-05-24
Online:
2022-08-13
Published:
2022-08-13
Contact:
Wei Wang
About author:
Wei Wang, wangw@imr.ac.cnXinlei Zhou, Bin Wang, Tianyi Zeng, Wei Yan, Junhua Luan, Wei Wang, Ke Yang, Zengbao Jiao. Effect of Pre-deformation on Nanoscale Precipitation and Hardness of a Maraging Stainless Steel[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(12): 2089-2100.
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Cr | Ni | Mo | Co | Ti | Fe |
---|---|---|---|---|---|
12.28 | 7.48 | 3.6 | 8.0 | 1.36 | Bal. |
Table 1 Chemical compositions of the experimental steel (H?+?O?+?N?<?0.0040 wt%)
Cr | Ni | Mo | Co | Ti | Fe |
---|---|---|---|---|---|
12.28 | 7.48 | 3.6 | 8.0 | 1.36 | Bal. |
Fig. 3 Optical and TEM images of the sample after solid solution treatment at 1050 °C for 1 h: a optical microstructure, b BF-TEM image and corresponding SAED pattern taken from the matrix oriented at [111] zone axis
Fig. 6 a, b BF-TEM images of S90 aged for 24 h, c corresponding SAED patterns taken from the matrix oriented at [011] zone axis, d BF-STEM image and STEM-EDS maps of Ni, Ti, Mo, Cr and Co
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1024 m−3) |
---|---|---|---|---|
US—1 h | 0.25 | 2.32 | 0.96 | 3.3 |
S90—1 h | 0.33 | 2.51 | 0.98 | 1.4 |
US—72 h | 0.55 | 6.0 | 2.14 | 8.3 |
S90—24 h | 0.65 | 4.80 | 1.6 | 12.9 |
Table 2 Rmin, Rmax, Rp and Nv of Ni3Ti precipitates in specimens with different RRs for different aging conditions
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1024 m−3) |
---|---|---|---|---|
US—1 h | 0.25 | 2.32 | 0.96 | 3.3 |
S90—1 h | 0.33 | 2.51 | 0.98 | 1.4 |
US—72 h | 0.55 | 6.0 | 2.14 | 8.3 |
S90—24 h | 0.65 | 4.80 | 1.6 | 12.9 |
Fig. 8 Isosurfaces of 6 at.% Mo concentration in different conditions: a US aged for 1 h, b S90 aged for 1 h, c proximity histograms of S90 aged for 1 h, isosurfaces of 6 at.% Mo concentration and 4 at.% Ni concentration plus proximity histograms of Ni3Ti and Mo-enriched precipitates in deformation d US aged for 72 h and e S90 aged for 24 h
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1022 m−3) |
---|---|---|---|---|
S90—1 h | 1.2 | 2.78 | 1.86 | 5.15 |
US—72 h | 2.88 | 6.03 | 4.68 | 13.26 |
S90—24 h | 1.31 | 5.31 | 2.01 | 9.78 |
Table 3 Rmin, Rmax, Rp and Nv of Mo-enriched precipitates in different specimens with different aging conditions
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1022 m−3) |
---|---|---|---|---|
S90—1 h | 1.2 | 2.78 | 1.86 | 5.15 |
US—72 h | 2.88 | 6.03 | 4.68 | 13.26 |
S90—24 h | 1.31 | 5.31 | 2.01 | 9.78 |
Fig. 9 a, b isosurfaces of 25 at.% Cr concentration in US and S90 aged for 1 h, respectively. c, d isosurfaces of 25 at.% Cr concentration plus proximity histograms of the Cr-enriched precipitates in US aged for 72 h and S90 aged for 24 h, respectively
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1024 m−3) |
---|---|---|---|---|
US—72 h | 1.31 | 7.93 | 3.86 | 1.10 |
S90—24 h | 1.37 | 5.99 | 3.00 | 1.33 |
Table 4 Rmin, Rmax, Rp and Nv of Cr-enriched precipitates in different condition specimens
No. | Rmin (nm) | Rmax (nm) | Rp (nm) | Nv (1024 m−3) |
---|---|---|---|---|
US—72 h | 1.31 | 7.93 | 3.86 | 1.10 |
S90—24 h | 1.37 | 5.99 | 3.00 | 1.33 |
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