Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (12): 2089-2100.DOI: 10.1007/s40195-022-01440-4

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Effect of Pre-deformation on Nanoscale Precipitation and Hardness of a Maraging Stainless Steel

Xinlei Zhou1,2, Bin Wang3, Tianyi Zeng1,2, Wei Yan2, Junhua Luan4, Wei Wang2(), Ke Yang2, Zengbao Jiao5   

  1. 1School of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 110016, China
    2Shi-Changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China
    3School of Material Science and Engineering, Zhengzhou University, Zhengzhou, 450001, China
    4Department of Materials Science and Engineering, City University of Hong Kong, Hong Kong, China
    5Department of Mechanical Engineering, The Hong Kong Polytechnic University, Hong Kong, China
  • Received:2022-04-12 Revised:2022-05-13 Accepted:2022-05-24 Online:2022-08-13 Published:2022-08-13
  • Contact: Wei Wang
  • About author:Wei Wang, wangw@imr.ac.cn

Abstract:

The effect of pre-deformation on nanoscale precipitates and hardness of a maraging stainless steel strengthened by the co-precipitation of Ni3Ti, Mo-enriched and Cr-enriched precipitates was systematically studied using electron back scattered diffraction, transmission electron microscopy and atom probe tomography (APT). Hardness measurements showed that the hardness of specimen with a deformation ratio of 90% peaked at HV 718 aged for 24 h, which is higher than that in the undeformed specimen (HV 603) aged for 72 h at 480 °C. APT characterization revealed that pre-deformation could shorten the incubation time of the Mo-enriched and Cr-enriched precipitates. At the early-aged stage, pre-deformation increased the stain energy that inhibited the nucleation of Ni3Ti precipitates, but accelerated the rejection of Mo from Ni-Ti clusters. Besides, the strengthening model indicated that strain hardening (43%) makes a larger contribution to the hardness at the early-aged condition, while precipitation hardening (58%) has most contribution to the hardness at the peak-aged conditition.

Key words: Maraging stainless steel, Pre-deformation, Precipitation hardening, Atom probe tomography