AN INCREMENTAL METHOD OF X-RAY DIFFRACTION QUANTITATIVE PHASE ANALYSIS OF SAMPLES CONTAINING AMORPHOUS MATERIAL

Abstract

Abstract: A new method for quantitative X-ray diffraction phase analysis of a powder misture has been developed according to Popovic's doping method. The weight fraction of amorphous material in the analysed sample is obtained. For a multicomponent system in which (n-2) pure phases are added into an n-phase compnent sample and theweight fractions of all n phases can be determined by the method. The test results of confirmation agree well with the theory.

Key words: X-ray diffraction, quantitative phase analysis, amorphous material, mass absorption coefficient

G. Chu(Department of Applied Chemistry Fushun Petroleum Institute, Fushun 113001, China). AN INCREMENTAL METHOD OF X-RAY DIFFRACTION QUANTITATIVE PHASE ANALYSIS OF SAMPLES CONTAINING AMORPHOUS MATERIAL[J]. Acta Metallurgica Sinica (English Letters), 1997, 10(1): 35-38.

[1]	Ibrahim Ondicho, Bernard Alunda, Dicken Owino, Luke Otieno, Melody Chepkoech. Revealing a Transformation-Induced Plasticity (TRIP) Phenomenon in a Medium-Entropy Alloy [J]. Acta Metallurgica Sinica (English Letters), 2020, 33(8): 1159-1165.
[2]	Wei Wang, Zong-Ning Chen, En-Yu Guo, Hui-Jun Kang, Yi Liu, Cun-Lei Zou, Ren-Geng Li, Guo-Mao Yin, Tong-Min Wang. Influence of Cryorolling on the Precipitation of Cu-Ni-Si Alloys: An In Situ X-ray Diffraction Study [J]. Acta Metallurgica Sinica (English Letters), 2018, 31(10): 1089-1097.
[3]	M. Santhiya, K.S. Pugazhvadivu, K. Tamilarasan, C. Rangasami. Influence of Sputtering Power on the Structure and Electrical Properties of Bi₂Fe₄O₉ Thin Films [J]. Acta Metallurgica Sinica (English Letters), 2017, 30(7): 650-658.
[4]	Ning-Ning Li,Min-Zhi Wang,Yong-Sheng Li,Guang Chen,Pei Li. Corrosion Behavior of Fe-Al Coatings Fabricated by Pack Aluminizing Method [J]. Acta Metallurgica Sinica (English Letters), 2016, 29(9): 813-819.
[5]	A. Harizi, M. Ben Rabeh, M. Kanzari. Substrate Temperature-Dependent Physical Properties of Thermally Evaporated Sn₄Sb₆S₁₃ Thin Films [J]. Acta Metallurgica Sinica (English Letters), 2016, 29(1): 79-88.
[6]	Rangasami Chinnusamy. Non-equilibrium Phases Formed in Cu-In-Se-Te System Synthesized by Melt-Quench Method [J]. Acta Metallurgica Sinica (English Letters), 2015, 28(5): 567-578.
[7]	Neena Bachan, A. Asha, W. Jothi Jeyarani, D. Arun Kumar, J. Merline Shyla. A Comparative Investigation on the Structural, Optical and Electrical Properties of SiO₂-Fe₃O₄ Core-Shell Nanostructures with Their Single Components [J]. Acta Metallurgica Sinica (English Letters), 2015, 28(11): 1317-1325.
[8]	Anuradha Purohit, Subhash Chander, Satya Pal Nehra, Mahendra Singh Dhaka. Thickness Dependent Physical Properties of Thermally Evaporated Nanocrystalline CdSe Thin Films [J]. Acta Metallurgica Sinica (English Letters), 2015, 28(10): 1299-1304.
[9]	K. Usharani, A. R. Balu. Structural, Optical, and Electrical Properties of Zn-Doped CdO Thin Films Fabricated by a Simplified Spray Pyrolysis Technique [J]. Acta Metallurgica Sinica (English Letters), 2015, 28(1): 64-71.
[10]	Sandip Sabale, Vishwajeet Khot, Vidhya Jadhav, Xiaoli Zhu, Yanhong Xu. Synthesis and Properties of Monodisperse Superparamagnetic Mg_0.8Mn_0.2Fe₂O₄ Nanoparticles Using Polyol Reflux Method [J]. Acta Metallurgica Sinica (English Letters), 2014, 27(6): 1122-1126.
[11]	Revathi V., Kumar S. Dinesh, Lekha P. Chithra, Subramanian V., Natarajan T. S., Muthamizhchelvan C.. Structural, Dielectric, and Magnetic Studies on Electrospun Magnesium Ferrite-Polyvinylidene Fluoride Core–Shell Composite Fibers [J]. Acta Metallurgica Sinica (English Letters), 2014, 27(4): 557-562.
[12]	Liu Yandong, Jiang Qiwu, Wang Yandong, Ren Yang, Tidu A., Zuo Liang. Goss Texture Evolution of Grain Oriented Silicon Steel by High-Energy X-ray Diffraction [J]. Acta Metallurgica Sinica (English Letters), 2014, 27(3): 530-533.
[13]	G.Chu, Y.F.Cong, H.J.You. MULTI-PEAK MATCH INTENSITY RATIO METHOD OF QUANTITATIVE X-RAY DIFFRACTION PHASE ANALYSIS [J]. Acta Metallurgica Sinica (English Letters), 2003, 16(6): 489-494 .
[14]	X.B.Qin, S.J.Cheng, X.F.Bian. MEDIUM-RANGE ORDER CLUSTERS IN Fe-2.0 ALLOY MELT [J]. Acta Metallurgica Sinica (English Letters), 2003, 16(6): 513-518 .
[15]	K.S. Guan. MONTE-CARLO SIMULATION FOR ATOMIC DEPOSITION OF AMORPHOUS ELECTROLESS Ni80P20 COATING [J]. Acta Metallurgica Sinica (English Letters), 2002, 15(5): 479-486 .

AN INCREMENTAL METHOD OF X-RAY DIFFRACTION QUANTITATIVE PHASE ANALYSIS OF SAMPLES CONTAINING AMORPHOUS MATERIAL

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments