Acta Metallurgica Sinica (English Letters) ›› 1999, Vol. 12 ›› Issue (5): 1180-1183.

• Research paper • Previous Articles     Next Articles

SYNTHESIS OF ULTRAFINE PLZT POWDER BY A SIMPLE CO- PRECIPITATION METHOD

H. Ying1) , X. D. Sun1) , Q. B. Yang1) , J. B. Li2) , Y. M. Wang2) , Z. Zhang3) and J. You3)1) School of Materials and Metallurgy , Northeastern University , Shenyang 110006 , China2) Departm ent of Materials , School of Mechanical Engineering , Shenyang University , Shenyang110044 , China3) Liaoning Analyzing and Testing Research Center , Shenyang 110015 , China   

  • Received:1999-10-25 Revised:1999-10-25 Online:1999-10-25 Published:2009-10-10

Abstract: Starting from cheap inorganic salts , ultrafine P L Z T po w ders were synthesized by a co pre cipitation m ethod . The results show that the precursor precipitate obtained by the co precipita tion method transfor ms co m pletely to P L Z T phase by calcining at 420 ℃ for 4 hours , about300 ℃low er than the nor m al transform ation te m perature of P L Z T obtained by m ixed oxidemethod . The effect of residual N H4 N O3 in the precursor precipitate on transfor m ation te m perature of the P L Z Tpow der w as investigated . The residual N H4 N O3 in the precursor po w der can reduce further the P L Z Ttransfor m ation tem perature to about 300 ℃, but a sm alla mount of Zr O2 and Pb Ti O3 re m ained . By a proper control of the synthesizing route , a P L Z T po w der with a pri m ary particle size of 10 n m and an agglom eration size of 0 3 μm hasbeen produced .

Key words: P L Z T, ultra fine po w der , co precipitation