Evolution of Annealing Twins and Recrystallization Texture in Thin-Walled Copper Tube During Heat Treatment

doi:10.1007/s40195-020-01090-4

金属学报英文版 ›› 2020, Vol. 33 ›› Issue (12): 1618-1626.DOI: 10.1007/s40195-020-01090-4

收稿日期:2020-01-05 修回日期:2020-02-25 接受日期:2020-04-01 出版日期:2020-12-10 发布日期:2020-12-11

Evolution of Annealing Twins and Recrystallization Texture in Thin-Walled Copper Tube During Heat Treatment

Song-Wei Wang¹^,², Hong-Wu Song¹, Yan Chen¹, Shi-Hong Zhang¹^,²(), Hai-Hong Li³

¹Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 110016, China
²School of Materials Science and Engineering, University of Science and Technology of China, Shenyang, 100049, China
³School of Nuclear Equipment and Nuclear Engineering, Yantai University, Yantai, 264005, China

Received:2020-01-05 Revised:2020-02-25 Accepted:2020-04-01 Online:2020-12-10 Published:2020-12-11
Contact: Shi-Hong Zhang

摘要/Abstract

Abstract:

Thin-walled copper tubes are usually produced by multi-pass float-plug drawing deformation. In general, the annealing treatment subsequently is necessary to release the stored energy and adjusts the microstructure. In this study, an investigation on the evolution of annealing twins as well as textures in the thin-walled (Ф6 mm×0.3 mm) copper tube underwent holding time-free heat treatment was reported. Electron backscattered diffraction analysis reveals that a large number of Σ3 boundaries (60° 〈111〉 twin relationship) are produced at the early stage of heat treatment, which is due to the lower boundary energy. With the recrystallization proceeding, the migration rate of grain boundaries decreases on account of the grain growth; meanwhile, the unique Σ9 boundaries (38.9° 〈110〉 relationship) are formed due to the interaction of the Σ3 boundaries. As a result, the number fractions of Σ3 boundaries and high-angle grain boundaries decrease rapidly. During the grain growth stage, a strong recrystallization texture was formed due to the fact that the grains of Goss orientation have a growth advantage over the others. As a result, the initial copper texture was transferred into the Goss texture in domination.

Key words: Copper tube, Annealing twin, Heat treatment, Electron backscattered diffraction (EBSD) analysis, Recrystallization texture

. [J]. 金属学报英文版, 2020, 33(12): 1618-1626.

Song-Wei Wang, Hong-Wu Song, Yan Chen, Shi-Hong Zhang, Hai-Hong Li. Evolution of Annealing Twins and Recrystallization Texture in Thin-Walled Copper Tube During Heat Treatment[J]. Acta Metallurgica Sinica (English Letters), 2020, 33(12): 1618-1626.

图/表 9

Fig. 1 Observation surface of the samples for EBSD measurement

Fig. 2 a EBSD orientation maps of the drawn tube, b texture components on (111) pole figure

Fig. 3 EBSD maps from the observation plane (DD-CD) of the tubes annealed at: a 200 °C, b 300 °C, c 400 °C, d 500 °C, e 700 °C, f 900 °C. Black lines and red lines show HAGBs and Σ3 boundaries, respectively

Fig. 4 Evolution of microstructural parameters for the tube samples during heat treatment

Fig. 5 (111) pole figure of samples at various annealing conditions: a 200 °C, b 300 °C, c 400 °C, d 500 °C, e 700 °C, f 900 °C

Fig. 6 EBSD map of the local position 1 in Fig. 3b: a the recrystallized grains, b the misorientation angle along the black arrow. The HAGBs and LAGBs are presented by black and gray lines, respectively

Fig. 7 Grain boundary map of the local position 2 in Fig. 3c. The HAGBs, Σ3, and Σ9 twin boundaries are represented by black, red, and pink lines, respectively

Fig. 8 Grain boundary map of the local position 3 in Fig. 3d. The HAGBs, Σ3, and Σ9 twin boundaries are represented by black, red, and pink lines, respectively

Fig. 9 IPF map and grain boundary map of the local Position 4 in Fig. 4e: a IPF, b grain boundary map. The HAGBs, LAGBs, and Σ3 twin boundaries are represented by black, white, and red lines, respectively

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Evolution of Annealing Twins and Recrystallization Texture in Thin-Walled Copper Tube During Heat Treatment

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