Acta Metallurgica Sinica (English Letters) ›› 2010, Vol. 23 ›› Issue (6): 473-480.DOI: 10.11890/1006-7191-106-473

• 研究论文 • 上一篇    

Oxidation behavior of TiAlZrCr/(Ti, Al, Zr, Cr) N gradient films deposited by multi-arc ion plating

赵时璐1,刘常升2,张钧3   

  1. 1. 东北大学；沈阳大学
    2. 东北大学材料与冶金学院
    3. 沈阳大学机械工程学院
  • 收稿日期:2009-10-10 修回日期:2010-03-01 出版日期:2010-12-25 发布日期:2010-12-14
  • 通讯作者: 赵时璐

Oxidation behavior of TiAlZrCr/(Ti,Al, Zr, Cr)N gradient films deposited by multi-arc ion plating

Shilu ZHAO1, Jun ZHANG1,Changsheng LIU2   

  1. 1) School of Mechanism Engineering, Shenyang University, Shenyang 110044, China
    2) Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, Northeastern University, Shenyang 110819, China
  • Received:2009-10-10 Revised:2010-03-01 Online:2010-12-25 Published:2010-12-14
  • Contact: Shilu ZHAO

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摘要： The Ti-Al-Zr target and pure Cr target were used to prepare the TiAlZrCr/(Ti, Al, Zr, Cr) N gradient films on the substrates of high speed steel (W18Cr4V) by multi-arc ion plating technique. Short-term isothermal (at 600oC, 700oC, 800oC and 900oC for 4h) and long-term cyclic (at 700oC and 800oC for 100h) high temperature oxidation behavior of the gradient film was studied. Scanning electron microscopy (SEM), energy dispersion X-ray spectroscopy (EDS) and X-ray diffraction (XRD) were carried out. It was showed that, under short-term isothermal condition, the high temperature oxidation resistance of the gradient film was excellent up to 800oC and an oxide scale comprising TiO2 was observed. On the other hand, under long-term cyclic high temperature condition, the oxidation resistance of the gradient film was excellent at about 700oC.

关键词: Multi-arc ion plating, TiAlZrCr/(Ti, Al, Zr, Cr) N gradient film, High speed steel, High temperature oxidation resistance

Abstract: The two Ti-Al-Zr targets and one pure Cr target were used to prepare the TiAlZrCr/(Ti, Al, Zr, Cr)N gradient films on high speed steel (W18Cr4V) substrates by multi-arc ion plating technique. Short-term isothermal (at 600℃, 700℃, 800℃ and 900℃ for 4h) and long-term cyclic (at 700℃ and 800℃ for 100h) high temperature oxidation behavior of the gradient films were studied. Then the oxide scales formed on the film specimens were characterized by scanning electron microscopy (SEM), energy dispersion X-ray spectroscopy (EDS) and X-ray diffraction (XRD). It was showed that, under short-term isothermal condition, the high temperature oxidation resistance of the gradient film was excellent up to 800℃ and an oxide scale comprising TiO2 was observed. On the other hand, under long-term cyclic high temperature condition, the oxidation resistance of the gradient film was excellent at about 700℃.

Key words: Multi-arc ion plating, TiAlZrCr/(Ti, Al, Zr, Cr)N gradient film, High speed steel, High temperature oxidation resistance