Acta Metallurgica Sinica (English Letters) ›› 2019, Vol. 32 ›› Issue (8): 951-960.DOI: 10.1007/s40195-018-00870-3

• Orginal Article • Previous Articles     Next Articles

Microstructural Evolution, Mechanical Properties and Thermal Stability of Gradient Structured Pure Nickel

Xiao Li1, Bo Guan2, Yun-Fei Jia1(), Yun-Chang Xin2, Cheng-Cheng Zhang3, Xian-Cheng Zhang1(), Shan-Tung Tu1   

  1. 1 Key Laboratory of Pressure Systems and Safety, Ministry of Education, School of Mechanical and Power Engineering,East China University of Science and Technology,Shanghai 200237, China
    2 School of Materials Science and Engineering, Chongqing University, Chongqing 400044, China
    3 AECC Commercial Aircraft Engine Co. LTD, Shanghai Engineering Research Center for Commercial Aircraft Engine, Shanghai 201108, China
  • Received:2018-10-11 Revised:2018-12-02 Online:2019-08-10 Published:2019-07-08

Abstract:

The microstructural evolution of pure nickel treated by deep rolling (DR) technique with different indent depths was investigated by means of optical microscopy and transmission electron microscopy. The surface roughness, hardness and residual stress distribution along the depth from surface were measured. Moreover, the DR-treated sample was annealed at temperatures from 300 to 700 °C for 2 h. The results reveal that dislocation movements are the fundamental mechanisms of gradient grain refinement during the DR process. With increasing indent depth of the DR, the gradient microhardness on the cross section of sample significantly increases, the maximum compressive residual stress decreases, and the affecting region of residual stress increases. The results of thermal stability depict that the microstructure can be stable as temperature up to 300 °C, and the abnormal grain growth and annealing twins are observed at 600 °C.

Key words: Deep rolling, Pure nickel, Microstructural evolution, Mechanical properties, Thermal, stability